Size by this method comes in micrometer, so can anyone suggest the solution how to get nano-sized particles and prevent aggregation?
This protocol may help you.
http://www.sciencedirect.com/science/article/pii/S0167577X05001539
Hydroxyapatite nano-particle can be otained by the controling the parameters of the precipitation process.
Well You can synthesize HAp nanofiber. Please refer to my paper
http://www.sciencedirect.com/science/article/pii/S0167577X14019491
They are stable for 6 months. Incase you specifically need nanoparticles try to change capping agent BSA would be good for this.
I hope this workout for you.
I recommend you this simple and well establish methodology:
https://www.researchgate.net/publication/230875618_Ion_exchange_behaviour_of_silver-doped_apatite_micro-and_nanoparticles_as_antibacterial_biomaterial
If you need more information contact me directly
Article Ion exchange behaviour of silver-doped apatite micro-and nan...
Thank you so much for your answers and articles
Problem concern is when ever I am dealing with particle size analysis by using DLS, size is not coming into nano. We require size of particles between 50-100 nm.
Well sir DLS is not correct way to measure size because it show hydrodynamic range
you should perform SEM or TEM analysis for exact size measurement.
And it may be possible that morphology of your particle is different that's why DLS is showing you size in higher range.
My suggestion is to perform SEM analysis.
All the Best
Thank You Akshay S Bhadwal for your corresponding reply. From SEM or TEM we will get to know the exact size of nanoparticles.
I have gone through some literature in which people are measuring particle size by using DLS and they are getting size properly.
I have suppose N samples of data obtained in an analysis and need to map into K (predefined) number of bins i.e. samples uniformly. For eg: I have N=31 and K=30 then i should have values of 1-14...
05 September 2016 3,577 3 View
In engineering strain we are consdering total or intial cross section area while in true strain it is instantaneous one.soif we measure strain using strain gauge then is it a true or engineering...
19 June 2015 3,393 4 View
Hi. Please tell me what guidelines should i need to follow for questionaries' type research work in India. It is not hospital based work, we are conduction basic institutional based qualitative...
03 March 2021 2,037 3 View
Need to image mesoporous silica nanoparticles using the TEM. Also, need high resolution TEM images to see the mesoporous structure. Kindly suggest what kind of grids to use. Thanks, Shatadru
02 March 2021 1,787 2 View
Hello all, I'm currently working on my undergraduate thesis and I'm having difficulties trying to access KLD Stats and Sustainalytics because my campus Airlangga University and apparently other...
02 March 2021 8,525 1 View
Hi everyone, I'm studying Marketing and I would like to write my PhD thesis on the topic of pricing. Any specific ideas?
02 March 2021 9,706 5 View
02 March 2021 3,060 3 View
02 March 2021 932 1 View
how to calculate BEHAVIOURAL REGULATION IN EXERCISE QUESTIONNAIRE BREQ 3 ,which contain 24 questions and each question has 5 answers (0- Strongly disagree , 1-disagree, 2- Neither agree nor...
02 March 2021 811 3 View
Please provide Book Title and author name
02 March 2021 9,059 3 View
An article that is published as a case study in the SJR listed journal. How much value is added to a researcher career? How it is evaluated by a scientific researcher/University admission...
02 March 2021 9,661 3 View
We have one plant, the local people using this for controlling blood sugar, the toxicity and antidiabetic activity of the plant is not reported yet, please guide from whag should be the process ?...
02 March 2021 2,300 1 View