I tried with some of the reported MOFs but there is a huge difference. Either there is a peak shift or there are alot of peaks. the peak shift is because of the stress and strain but too many peaks suggest different phases, but how can we identify them?
Dear Shoaib,
Try washing/purifying your product before characterizing. Are there any physical differences in the structure or appearance of products formed? If so try to separate them.
Regards,
Vincent Adimula
Hi Hamada,
Thank you for your answer
so yes i did prepared some reported MOFs, but i prepared them in a different solvent and different conditions. in general i prepared zinc imidazolate frameworkby only using imidazole.
So there are some peak shifts, lets suppose if reported peak is at 20° the measured peak comes at 21°. why does this small change occur?
Thank you
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