In other words, how to separate NIPAM monomers from PtBA-b-PNIPAM after copolymerization?
I've already precipitated in cold hexane, monomers are still there though.
Dialysis against H2O and then lyophilization can remove monomers.
You may want to try soxhlet extraction. You should check properly the solvents that don't dissolve your block. It may be a method to decrease PDI as well.
Regards,
Patricia
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