I prepared a MOF, ZIF through solvothermal method. I run the cyclic voltametry with following conditions. I opted the conditions from the literature.
Electrodes : Glassy carbon electrode (WE), Graphite (CE), AgCl (RE)
Electrolyte : Phosphate buffer
But the peaks started diminishing after few cycles, say around 20 cycles. I understood this is because the electrochemical cycling stability of MOF is lesser. I would like to know how the electrochemical stability of the MOFs can be improved via some means. Thank you.