I'm currently doing my master's final year internship and I'm aiming to model the rheoloical behaviour of polymer solutions as a function of various parameters such as the temperature and the shear rate. My experimental approach includes measuring the viscosity of the semi-dilute solutions using a cone-plate rheometer. When I started the first batch of solutions (concentrated from 3 to 8%), I used a 60mm/1° cone. However, as I reached 8% of concentration, I got the torque overload error because my solutions strated being too viscous so the 60mm cone was not adequate to measure their viscosity. Therefore, I had to use another geometry and following the operational mode of the equipment, if I get the "torque overload" issue, I have to use the Plate-Plate 35mm. In order to verify that changing the geometry will only allow me to conduct the measurment without actually affecting my results, I measured the viscosity of a sample from the first batch (3 to 8%) with this new geometry and to my surprise, the results did change compared to those that I got using the 60mm cone even though I put the right reference of each geometry on the software. I then tried with other cones with different diameters and angles and they all gave different results. Could anyone help me with this matter ? What could be the possible reasons behind this ? Does the cone geometry influence the measured viscosity ?

Thank you,

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