21 October 2014 0 8K Report

Does someone have experience using methyl orange to monitor silylation by MSTFA? I found an old article by Donike (Journal of Chromatography, 115 (1975) 591-595) proposing the addition of a small amount of methyl orange solution to the silylation medium in order to monitor the completeness of the reaction. Nevertheless I couldn't find any article using this technique.

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