Measurement results with angle range -60° to + 60° varries considerably when measure with 0 to 60°.
the latter measures 50 MPa more than the former
hi,
which angle you measuring? si or fi
how about your device? is it have a goniometer?
fi angle is important to calculate. if your cathode tube have a filter. under 60 and maximum peak is good and no problem on your measuring.
if dont have filter you must use about 60 degree angel.
si angle need for better results.
is your device calibrate?
to get more information read book of sir fitzpatrik. he has agood book to guidance x-ray measuring.
this file i upload is a best refrence to use and get you information.
That make sense since the measured stress depends of the hkl planes
Regards,
Pedro
Thanks Mr. Pedro. Could you please explain a little more
hi
as i know hkl is arrow of crystalization. it seems that change the your crystalzation plane change your parameters.
thats true. but not for this. its one of many reasones.
stress change when your atomic distance change.
x ray shows you the diffrent of the martial whithout stress against the matial from change strain on it.
strees= d1-d0/ E
d mean atomic distance
E= young madulus
when your angles change that results maybe your crystalization plan change but 50 Mpa is very big for this.
i dont know exactly what change on your duties. that guidance show you more information.
that is i know about this methode.
Require for Rietveld refinement in XRD.
08 August 2024 3,081 2 View
During low-temperature testing, new diffraction peaks that appear could be indicative of several phenomena. In one of our tests, we observed notable new peaks around 40° and 45° in a specific...
06 August 2024 726 3 View
I want to refine one XRD peak of my in-situ xrd but the background is never working good which ultimately fails the refinement. How to refine and adjust the background using GSAS-II
05 August 2024 5,291 2 View
What is the role of oxidative stress in toxin-induced carcinogenesis? I am currently researching the impact of environmental toxins on children's health and would greatly appreciate insights from...
02 August 2024 3,174 1 View
How to calculate the molar proportions of the oxides from the XRF analyses?
02 August 2024 2,565 2 View
I fabricated Ti3C2Tx using concentrated HF 40%, I plot an XRD as attached image below.. please let to know if I obtained it or not.
02 August 2024 6,789 4 View
What information we can get from PXRD analysis other than from SCXRD analysis of a crystal ?
30 July 2024 6,261 4 View
I will be doing an XRD on a sample which is powdered in natured and is a hydrogenated compound. I would like to know how we can understand the individual components and components by using the...
28 July 2024 4,548 2 View
i compare between the antioxidant and oxidative stress level between negative control rats (saline) and CCL4 intoxicated rats. i found the level of GSH and TAC is more in toxic group than normal....
26 July 2024 1,887 0 View
The aim of the research here is to prevent the propagation of the crack in the fabricated elastic medium with useful applications.
25 July 2024 9,976 3 View