I mean what should be the ppm level to get a calibration curve. I tried but more than 10ppm the complex is very weak and gradually disappears. Any comment/suggestion is appreciated.
For your information, for more than 1 ppm Cr(VI) there is no need to use DPC. You can directly measure the concentration using a UV/Vis spectroscopy. However, if you are eager to use DPC, the above mentioned papers are useful.