While getting a result from XRD single crystalline data, how do I identify the result match with the expected compound. Is there free data available?
Respectful Researchers, Can any one please help me to calculate the area II (green color) using origin and / or available software.How can i exact the charge and discharge values from this P - E...
07 August 2018 7,075 2 View
respected researcher, recently i examine the pelletised powder sample( rare earth doped BiFeO3)in PE loop tracer under room temperature the Pmax is 0.352micro coloumb / cm2. then i pool the...
05 June 2016 4,141 0 View
I am attaching here DSC results of my powder sample. The following are the details of the sample. 1.the sample mass (13.190mg) 2. heating rate (10deg/min) 3. range (-100 to 500c) output files...
11 December 2014 2,664 13 View
For example, if we take the FTIR result of BiFeO3 powder sample, I get peaks at 449.80cm-1 & 593.14cm-1 which conforms the presence of O - Fe - O bending mode and Fe - O stretching mode ( Ref:...
09 October 2014 4,937 4 View
From the data of wavenumber vs absorbance from FTIR, i find that there are some peaks. from that, the wavelength and angular frequency of the BiFeO3 are calculated , also mass of the Bi, Fe and O...
08 September 2014 1,483 1 View
I have grown a Bismuth ferrite sample through solid state and I observed that there are some secondary phases due to iron sillenite (Bi25FeO40). I am in need of Bi25FeO40 CIF file to refine the...
01 February 2014 7,099 4 View
Require for Rietveld refinement in XRD.
08 August 2024 3,080 2 View
During low-temperature testing, new diffraction peaks that appear could be indicative of several phenomena. In one of our tests, we observed notable new peaks around 40° and 45° in a specific...
06 August 2024 724 3 View
I want to refine one XRD peak of my in-situ xrd but the background is never working good which ultimately fails the refinement. How to refine and adjust the background using GSAS-II
05 August 2024 5,288 2 View
How to calculate the molar proportions of the oxides from the XRF analyses?
02 August 2024 2,558 2 View
I fabricated Ti3C2Tx using concentrated HF 40%, I plot an XRD as attached image below.. please let to know if I obtained it or not.
02 August 2024 6,788 4 View
What information we can get from PXRD analysis other than from SCXRD analysis of a crystal ?
30 July 2024 6,259 4 View
I will be doing an XRD on a sample which is powdered in natured and is a hydrogenated compound. I would like to know how we can understand the individual components and components by using the...
28 July 2024 4,547 2 View
I'm working with a hydrogel sample and I'd like to perform XRD analysis. Can anyone offer guidance on preparing the hydrogel for the XRD instrument? Specifically, I'm unsure about the best method...
20 July 2024 3,609 4 View
Can we measure the 2θ variation within a 5-degree range on a Bruker D2 Phaser XRD machine? I have experienced problems with diffraction angles (2θ) below 10 degrees. Is this range within the...
13 July 2024 2,615 4 View
XRD analysis
08 July 2024 977 4 View