can we prepare Tin sulfide in ball milling by directly mixing Tin powder with the sulfur in control atmosphere with argon gas?
Hi Smit: My suggestion is to ask this question to any site in the web that is able to search (e.g. google and many others). You will get thousands of answers within seconds. You just have to read......
The second way to get an answer is to go to your lab and try the reaction. Then you will see.
Such questions are really annoying!
Hi Smit: My suggestion is to ask this question to any site in the web that is able to search (e.g. google and many others). You will get thousands of answers within seconds. You just have to read......
The second way to get an answer is to go to your lab and try the reaction. Then you will see.
Such questions are really annoying!
I think using ball milling you will mix the components very well, but the reactions needs to be initiated (thermally). So after milling, you should heat the mixture. This could be a very exothermic reaction which may lead to a thermal explosion (careful I). It may be safer to initiate the powder only locally and have the reaction front run freely through the mixture (Self-sustained High-T Synthesis).
I think it is possible, but you have to use high-energy milling techniques. See the following publications:
- Takuya Tsuzuki, Paul G. McCormick, Mechanochemical synthesis of metal sulphide nanoparticles, Nanostructured Materials Volume 12, Issues 1–4, 1999, Pages 75-78
- A. Bakhshai, V. Soika, M.A. Susol, L. Takacs, Mechanochemical Reactions in the Sn–Zn–S System: Further Studies, Journal of Solid State Chemistry Volume 153, Issue 2, September 2000, Pages 371-380
- L. Takacs, M.A. Susol, Gradual and Combustive Mechanochemical Reactions in the Sn–Zn–S System, Journal of Solid State Chemistry Volume 121, Issue 2, 1 February 1996, Pages 394-399
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