Can anyone suggest me a TLC solvents system for cubenol. and any related paper of purification of cubenol from plant extracts (it is sesquiterpinoid)?

More Ashwini Murthy's questions See All

Which stain is used to see the deposition of oil or oil glands in anatomy section of leaf(transverse section) in cymbopogon?

Cymbopogon is an aromatic grass which produces essential oils as a secondary metabolite so to see the deposition of oil in leaves transverse section of intra and inter species can you suggest me...

07 August 2019 7,607 2 View

Extraction and characterization of plant Antimicrobial peptides?

I am extracting proteins from plant leaf samples by using Tris EDTA method but the problem is I am getting protein but on running sample on SDS PAGE of 15% gel I m not getting clear bands either...

04 May 2019 9,428 9 View

Can anyone refer me list of terpene and terpenoid with their Rf values?

I am doing tlc of cymbopogon martini leaves extract (methanol chloroform and Ethyl acetate extract ) can anyone suggest me papers for identifying compounds (terpenoid compounds) with their rf values

11 December 2018 5,166 3 View

Polymer composites suddenly solidifies?

I am making polymer composite by solvent mixing method. When I am trying to add filler solution in polymer solution it quickly get solidified. How to make them then uinform? It doesn't give time...

03 March 2021 7,540 4 View

What solvent can I used for Paal Knorr reaction between 6-amino hexanoic acid and 2.5 hexanedione?

I am try to make the Paal Knorr reaction between 2.5 hexnedione and 6-amino hexanoic acid, my problem is type of solvent to use, because 6-hexaminohexanoic acid is soluble in water but I am not...

02 March 2021 4,443 2 View

Waters 2707 HPLC autosampler problem?

I am using a 2707 waters HPLC device. When I try to inject a sample, it says missing plate or rack. I changed the needle and calibrated its position but I still get the same problem. I even get...

02 March 2021 1,408 1 View

How to polymerize TEOS?

I want to polymerize TEOS on a surface. I know that NH4OH is a preferred catalyst and an alcoholic solvent should be used .But I can not find certain amounts of each material to use. Does any one...

02 March 2021 1,404 6 View

How optimize the Size Exclusion Chromatography?

Hello! I'll do a size exclusion chromatography, but I only have an open column, and I'll perform the peptide extraction from yeast, using buffer lysis (sodium phosphate 50 mM/NaCl 30 mM/DNAse and...

01 March 2021 2,215 2 View

How can extract ciprofloxacin hydrochloride disolve in water er to organic solvent such as dichloromethan or any other solvent?

I need a procedure to extract the ciprofloxacin hydrochloride from aqueous solution by using dichloromethane in detail,. I thank you very much.

01 March 2021 4,306 1 View

How to separate water from glycerol solvent in a solvent recovery vacuum distillation column?

I am currently doing my third year design project. I have been assigned to design a glycerol recovery column in vinyl acetate monomer production. The process unit before the recovery column is an...

01 March 2021 9,525 4 View

Precipitate after adding laemmli buffer to protein solution containing Potassium Acetate?

Hi, I am running a size exclusion chromatography experiment with a buffer containing Potassium Acetate as a salt. I analyse these fractions through SDS-PAGE. After boiling my SEC fractions in...

01 March 2021 2,622 3 View

Any research papers for extraction of nutrient deprivation on macroalgae? Analysed by HPLC-UV and GC/MS. Possibly from macroalgae genus Rhizoclonium?

I am doing my thesis on the nutrient deprivation on the macroalgae Rhizoclonium sp. I will be analysing the levels over a period of roughly 5 days by HPLC-UV and GC/MS. I will be using seawater as...

28 February 2021 6,477 1 View

Are protein samples in SDS compatible with ELISA?

I have used an AllPrep DNA/RNA/Protein Mini Kit QIAGEN kit to extract RNA and protein from my samples. At the end of the protein purification, I resuspend my protein in 5% SDS. Will these samples...

28 February 2021 7,370 3 View

Karen A. Darbinyan Popular answer

Hello, see below info may be useful for you.

https://www.researchgate.net/publication/269754896_TLC_of_selected_sesquiterpenoids_of_the_Asteraceae_family

Good luck!

Karen A. Darbinyan

Ali Alsuraifi

https://pdfs.semanticscholar.org/d2b6/b5620bae57ce3c7eebca8d04c453c133cd9f.pdf?_ga=2.132369358.1986456121.1546074220-575847691.1546074220

Jack Silver

Article The structure of cubenol and epi-cubenol

They purified the compound on silica, the solvent system for silica purification will work for TLC.