Try one experiment with reverse addition i.e., charge solvent in the beaker and add reaction mass.

Kishore Kumar Sriramoju Can you provide me with some more info on how to do this?

First dissolve compound/material in X type solvent. Add this solution to antisolvent (Y type) to crystallize the material. Vary the addition time, addition temperature and RPM (mixing) to get different size of particles.

Hello

I don't know what method and materials you use, but I can give you some general advice.

First, refer to similar articles or theses or patents, depending on the topic of your work, where you can get more information from their experimental section. In the next step, categorize them, that is, filter your information based on what you want.

Second, use relevant keywords to search.

Third, after filtering the information, you can also get advice from people whose work is very similar to yours.

I have included articles here as examples that I hope will be useful to you.

Review on Additive Manufacturing of Single-Crystal Nickel-based Superalloys

Three-Step Mechanism of Antisolvent Crystallization

Using AntiSolvent For Crystallization

https://www.mt.com/hr/hr/home/applications/L1_AutoChem_Applications/L2_Crystallization/recrystallization.html#:~:text=Recrystallization-,Recrystallization,Optimization%20of%20Crystal%20Properties%20and%20Process%20Performance,-Zatra%C5%BEite%20informacije

Synthesis, Crystal Structure and Thermal Properties of Lead(II) Complex with Bathophenanthroline and Benzoyltrifluoroacetonate Ligands

Synthesis and characterization of lead(II) complexes with substituted 2,2′-bipyridines, trifluoroacetate, and furoyltrifluoroacetonate

Method for producing single crystal, and needle-like single crystal

https://www.mdpi.com/journal/crystals/special_issues/Anti-Solvent_Crystallization

A novel mechanism to generate metallic single crystals

What type of Material you want to grow using the Anti solvent method? Depend upon the materials I can suggest you. Is it a MO?