i am doing reaction both material inTHF and my product also must dissolve in THF or not?
my compound is anime and silicon containing compound this compound can't dissolved any other solvent such alcohols,THF,CHCl3 this much solvent ?
give some suggestion which solvent i will be using that compound dissolved?
Ankita Ray
You have not mentioned how polar or non-polar your compound is. Try using DMSO or pyridine. If its broadly polar, maybe you can measure your proton NMR with DMSO or pyridine.
Have you tried a mixture of benzene and diethyl ether? These would be my go to solvents when the Rf value while running a TLC is not more than 0.2 using the eluent system DCM:MeOH 10%
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