Rakesh Madri

5 Questions 5 Answers 0 Followers

Questions related from Rakesh Madri

How are the silane solution stabilised?

Dear all, we know that silanes are prone to hydrolysis, hence if one wish to store a silane solution say 2% , how can we acheive this. I guess that we must have a properly dry solvent free from...

28 September 2023 9,387 1 View

Can triethylamine be used as a base in refluxing toluene or DMF?

As the boiling point of TEA is ~ 90 ᴼC, I guess that on using refluxing toluene or DMF, TEA will remain in vapor phase above the surface of the solvent and so it will not act as a base in a...

07 March 2019 4,403 0 View

How to selectively protect the e-amino group in lysine?

dear all can anyone help be in selectively protecting the e-amino group in lysine as I wish to perform acylation of a-amino group iin lysine .

23 April 2017 2,979 5 View

Can anyone suggest me a way to synthesize monoamide?

I wish to synthesize mono amide of carboxylic acid. For this i am trying to partial esterify the diacid followed by reacting the monoacid with amine but i got diester and very small quantity...

09 March 2016 9,077 3 View

How can we take the NMR of a moisture sensitive compound?

I wish to take NMR of Ethyl 6-(chlorocarbonyl)-pyridine-2-carboxylate

03 September 2015 971 4 View