Hi guys,

I have prepared the small Mn3O4 NPs via the method reported in the literature.

Details of the synthesis are as follows:

300 mg Mn(acac)2 and 9.63 ml oleylamine were heated at 150 ℃ for 9 h under an N2 atmosphere. After the product cooled to room temperature,excess ethanol was added to obtain precipitates.

Why are there many large particles in the TEM images?

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