What is potentail window of Selenium in HClo4 electrolyte using Glassy Carbon Electrode?

05 May 2016 1 2K Report

I am trying to detect Selenium (IV) using Glassy Carbon electrode in perchloric acid but not able to observe any oxidation/reduction peak for selenium (IV) in cyclic voltammogram (CV: range -1 to 1). Could anyone suggest any solution for it.

Cornel Radu

I suggest you to read this paper (pag.75):

http://cordis.europa.eu/pub/fp7/euratom-fission/docs/recosy-firstannualworkshopproceedings.pdf

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