I am trying to prepare titanium isoproxide nanoparticles using plant extract, but when I trying to characterize them in full scan UV-Vis mode my peak did not come. it comes in 222nm. Even I diluted the sample.
Titanium isoproxide nanoparticles cannot be obtained by your method. Their melting point is 14-17 degrees. The maximum in the spectrum is observed from the substances of your extract.
I have hereby attached the pic of my purchased Titanium isoproxide as well as the papers from where I am following the literature.
We are using root extract and everything done according to attached paper. Even our root extract do not give visible range wavelength. We also use the scan wavelength as mentioned in the paper. For root extract preparation I am using another paper also attached.
What do you mean by the synthesis description. I a using the same protocol. But still not getting results. Because in the paper they are using titanium isopropoxide.
Yuri Mirgorod is being very patient with you. You state in your question: 'I 'm trying to prepare titanium isoproxide nanoparticles'.
This is not the case and confusing. You are preparing TiO2 nanoparticles (or trying to prepare) from titanium isopropoxide precursor. I did exactly the same in my Ph.D.
I suspect that your conditions are not correct for the production of TiO2. Indeed I do not understand the need for a 'plant extract' given that it's the hydrolysis of titanium isopropoxide that is used for TiO2 production. The major reason for using titanium isopropoxide is that it is soluble in alcohols and addition to alkaline aqueous media precipitates the TiO2 (or Ti(OH)4, if I'm pedantic).
I completely understand your answer, but tell me how should I prepare the nanoparticles using Titanium Ispordxide as precursor of course it will be TiO2.
I am following the same methods.
I completely understand your answer, but tell me how should I prepare the nanoparticles using Titanium Ispordxide as precursor of course it will be TiO2.