During the hydrosilylation process, silicon nano-particles get polymerized and it is very difficult to process further. Is there any suggestion to avoid polymerization.
Can you please identify/explain the solvent system for dispersion of silicon nanoparticles?
Different solvents, depending upon the nature of desired fictionalizations.
by heating at moderate temperatures. Also vacuum drying is applied but same results
Could be the moisture problem. Try with dry silica gel, especially the one with the moisture indicator. Keep some time in closed vessel with the solvent, then decant carefully. Works well.
the solvent was already placed inside desiccator while applying vacuum pump. On the other hand the thermal drying was executed inside glovebox having
One of the options is to subject the hydrogen-terminated silicon nanoparticles to hydrosilylation added upon by a hydrosilylating reagent and brought about by microwave radiation.
Mr. Kulkarni,
Can you please explain the method your are describing ?
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