I am using a published pulse sequence from Chem Eur. J. (DOI: 10.1002//chem.201201577) for 1D HOESY. The sample has two F separated by 3 ppm. I have attached the 1H spectrum where I can see NOE but can't properly phase the peaks. I have tried the obvious fixes to no avail. Any suggestions? Also, I can't seem to change the pulse shape when executing this sequence. I have also attached the pulse sequence if that helps.

Thanks, Bill

More William Brittain's questions See All
Similar questions and discussions