How to prepare isobutyric acid:H2O:ammonium hydroxide v/v/v (66:33:1) solution?

07 June 2021 0 3K Report

I tried to prepare this solution, but I may be mistaking, as my experiment result doesn't seem to be Ok. So please correct me if I am wrong.

So I needed to prepare isobutyric acid:H2O:ammonium hydroxide v/v/v (66:33:1) solution.

I took isobutyric acid (>98% pureness) 33 ml, water 16.5 ml and 0.5 ml of ammonium hydroxide

from 1 mol/liter ammonium solution. I guess I may be mistaking in ammonium hydroxide here.

Does anyone have an idea?

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