Would you tell me how to measure the stacking fault energy of face-centered cubic structured metals and alloys by experiment? Especially, I would like not to use a transmission electron microscope. The simplest method possible is preferable.
X-Ray Diffraction along with Rietveld refinement technique could be used to find the SFE of metals. This has already been reported in the case of Cu.
References:
* Stobbs WM, Sworn CH The weak beam technique as applied to the determination of the stacking-fault energy of copper. Philos Mag 24(192):1365–1381, (1971)
* Reed RP Relationship between stacking-fault energy and x-ray measurements of stacking-fault probability and microstrain. J Appl Phys 45(11):4705–4728, (1974)
Indeed، one can determine the width of the SF by X-Ray Diffraction.Subdequently ,one can measure the SFE from the width of the SF. The higher the SFE the smaller the width of the SF the easier for the SF to slip .ln contrast,the lower the SFE the bigger the width of the SF the harder for the SF to glide.