Hello all,
I have prepared an imine but I am not able to isolate it purely.
In acidic silica it gets decomposed and I can not distil it because it's a small scale reaction and I am getting total 4 spots.
In basic alumina imine is coming in 1-2 % EtOAc+Pet ether but along with that one of my starting material is also coming which is highly nonpolar.
Kindly suggest any other method of isolation of imine.