how to characterized whether Fe3O4 or Fe2O3 is formed by reacting FeCl3.6H2O and FeCl2.4H2O(2:1) in the basic medium under a nitrogen atmosphere?
will it be characterized by using IR or UV spectroscopy?
It is anticipated that you could be able to distinguish them by Raman. You could also be able to find residual starting materials, if applicable, by Raman Micro-Analysis.
https://www.researchgate.net/post/How_to_distinguish_between_Fe3O4_and_g-Fe2O3
Follow this link.
How about trying X-ray ( or electron) diffraction?
Best wishes,
Carlos
By Mossbauer spectroscopy, one can determine the oxidation state of iron.
Sandip Munshi Dear sir, in both Fe3O4 and Fe2O3, Fe will be in both oxidation states that is Fe+2 and Fe+3.
You can carry out the powder XRD (pXRD) experiment Vikas Yadav
Sandip Munshi thank you for your suggestion sir
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