I have read about it's generation from sodium sulfide. But I don't get the exact procedure for hydrogen sulfide generation and also about determining its concentration. Is there any other method?
Almost all surfur compuunds may generate HS when add acid. HCL for example.
You can generate sulfide (H2S) by reacting iron sulfide with hydraulic acid (HCl). The reaction products will be iron chloride and H2S.
I teach this approach in my chemical engineering teaching laboratory at Yale University.
Hope this helps answer your question.
Professor Yehia Khalil
Yale University
USA
I need to know the concentration i am adding each time.
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