My emulsions (olive oil in 30 mM NaCl) are expected to have droplet sizes of 5-10 µm. I ran through a Mastersizer 3000, dispersing it in 30 mM NaCl. However, I got distribution of size of 100 µm too.

Did anybody face similar issues?

I read through Malvern manuals, it is recommended to pre-dilute the emulsions before running through the Mastersizer 3000.

How do we do this?

Thanks

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