I am doing a study on Dry matter and TSS prediction of multi-year fruit NIRS spectra. I want to develop calibration model of DM and TSS separately for each year using PLS tool box. I have created separate spectral and DM/TSS parameter for each year in same matlab file. While feeding the parameter in Y box of PLS tool box I could not find more than 4 parameters of TSS and no DM parameter showed up. Could any body tell me how could I resolve this issue or there is any limitation on number of Y variable in PLS toolbox?

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