In TiO2 films, which are often sintered at 450°C for 30 or 60 minutes for application in dye-sensitized solar cells (DSSCs), show no appreciable connectivity between the TiO2 particles. The electrode sintered at a temperature of 450°C shows a higher photocurrent attributed to the formation of the higher crystalline film. This enhancement in the interconnection between particles results in a swift diffusion of electrolytes and good transportation of electrons in the film. For example, TiO2 films sintered at higher temperatures (700°C) but for a shorter time (10 min) exhibited better connectivity between the particles with a slight reduction in surface area. For more details read the following references;
Article Effect of Sintering Profiles on Titania Interparticle Connec...
Article Effect of counter electrode, thickness and sintering tempera...
thanks so much, Mahmood H. M. but what about if I heat or increase the temperatures overall the system (testing temperatures), not reaction temperature
Increasing the temperatures of the overall testing system may cause side effects on the process. but , you can try to study this cairfully. hope you get good results.