To know the phase for example
You have to increase the collection time to get better XRD pattern. You can't use this XRD pattern for further analysis.
Hello!
The good way to analyze this XRD and to have a rough idea about phase and other parameters I'd suggest to carry out analysis using X'pert High-score software. It will give a rough idea about different parameters.
Hello!!
What type of sample are you using? Is it a polymer sample?
I feel you can take care of these points:
1. Fill your sample fully on the sample holder (Hump in pattern may be because of glassy sample holder).
2. Take scan in the range of two theta from 10 to 70 degree.
3. Record the data for longer time say 1 degree per minute.
Only then go for processing the obtained pattern for any analysis.
Thank you very much
How to start up to write an article
03 April 2018 7,431 7 View
By using SEM technique for example
02 March 2018 5,531 10 View
Require for Rietveld refinement in XRD.
08 August 2024 3,081 2 View
During low-temperature testing, new diffraction peaks that appear could be indicative of several phenomena. In one of our tests, we observed notable new peaks around 40° and 45° in a specific...
06 August 2024 726 3 View
I want to refine one XRD peak of my in-situ xrd but the background is never working good which ultimately fails the refinement. How to refine and adjust the background using GSAS-II
05 August 2024 5,291 2 View
How to calculate the molar proportions of the oxides from the XRF analyses?
02 August 2024 2,565 2 View
I fabricated Ti3C2Tx using concentrated HF 40%, I plot an XRD as attached image below.. please let to know if I obtained it or not.
02 August 2024 6,789 4 View
What information we can get from PXRD analysis other than from SCXRD analysis of a crystal ?
30 July 2024 6,261 4 View
I will be doing an XRD on a sample which is powdered in natured and is a hydrogenated compound. I would like to know how we can understand the individual components and components by using the...
28 July 2024 4,548 2 View
I'm working with a hydrogel sample and I'd like to perform XRD analysis. Can anyone offer guidance on preparing the hydrogel for the XRD instrument? Specifically, I'm unsure about the best method...
20 July 2024 3,611 4 View
Can we measure the 2θ variation within a 5-degree range on a Bruker D2 Phaser XRD machine? I have experienced problems with diffraction angles (2θ) below 10 degrees. Is this range within the...
13 July 2024 2,615 4 View
XRD analysis
08 July 2024 977 4 View