I want to use this powder to impregnate it in multi walled carbon nanotubes.
Here is a US Patent, describing it:
http://www.freepatentsonline.com/3959453.html
And, by the way, this is a good idea for an electroanalytical process!
Electrochemical preparation of PbO2 is well-known , you can use it to get a thick plate that can be crushed into the desired particle size
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