The metal core capillary tubes of Electrospinning were clogged with PVA/chitosan polymer. We soaked it in hot water and acetic acid solution (%5), but there was no change. How can we dissolve this polymer?
The clogging of the capillary tubes in electrospinning can be a common issue, and the method you tried (soaking in hot water and acetic acid solution) may not be effective for dissolving PVA/chitosan polymers. Here are a few alternatives to consider:
Use a stronger solvent: Try soaking the tubes in a stronger solvent such as ethanol or dimethyl sulfoxide (DMSO). These solvents may be more effective in dissolving the PVA/chitosan polymer.
Incorporate a plasticizer: Consider adding a plasticizer, such as glycerol, to the polymer solution before electrospinning. This can help prevent clogging and make it easier to clean the tubes.
Increase the temperature: Increase the temperature of the hot water and acetic acid solution to near boiling point and prolong the soaking time to try to dissolve the polymer.
Use ultrasonic cleaning: Try using ultrasonic cleaning in a mixture of water and acetic acid to agitate and remove the polymer.
We tried increase the temperature of hot water and acetic acid solution but there was no change. Also we tried soaking the tube to DMSO solvent, there was a little dissolve. Now we are trying soaking the tube to %5 H2SO4 solution. I hope it can dissolve.