befor starting the test, my sample is white and when i finish the test it turn to black and after a few hours it turns to the initial color (white) .... do you have any explanation for that ?
The attached reference might be helpful for your question. Good luck.
TiO2 is being grey color under inert gas with using alcohol......
Thank you Suresh Thangudu & Luma M. Ahmed for your help !
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