If I have a complex connected with another ligand by a hydrogen bond with coordinated water from that complex; is this H-bond effect on the range of losing the coordinated water until 210 C because I have it? I need references, please.
Hello.
In the literature there are at least 2 references, the closest to the topic you are proposing, which are shown below:
Kawakami, Kohsaku. "Pharmaceutical Applications of Thermal Analysis." Handbook of Thermal Analysis and Calorimetry. Vol. 6. Elsevier Science BV, 2018. 613-641.
Galwey, Andrew. "Dehydration of Crystalline Hydrates." Handbook of Thermal Analysis and Calorimetry. Vol. 2. Elsevier Science BV, 2003. 595-656.
Dear dr.
I guess that the answer is not straightforward, first you have to detect the mechanism in each stage of TGA, find the first and second derivatives and try to obtain the product at 210C and do MS (mass Spectroscopy) and IR, i.e. Monitoring the product at different stages, but don't forget removing the water attached to the crystal surface by leaving the product 48hr in a 60C oven
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