The Reaction mixture is on stirring from more than two weeks, TLC showing the spot of product. But product is not extracting out.
Jorge alejandro Tapia
@Syeda It would be necessary to know the desired reagents and products to generate a more adequate answer.
Oily mixtures tend to be mixtures of several compounds. It would depend on the amount of compounds observed and their RF the method of separation. In case you are sure that you have obtained the desired majority product, HPLC or column chromatography would be the most appropriate. Subsequently recrystallize the product.
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Chen Jingwen
Hi,
The following steps may help you:
1. Select appropriate reagents so that they can form salts.
2. Perform vacuum distillation
3. Purification using column chromatography
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