I want to do electro polymerization of pyrrole on graphite sheet through chronoamerometry with nova software but l do not know how values should be filled in software for this method . Secondly when l try.with CV then electro polymerization was done on platinum counter electrode
Confirm whether you are trying to deposit polypyrrole galvanostatically using Autolab Nova? Also, for CV, try reversing the connections of counter and working electrodes i think u have connected those wrongly.