Sujoy Sarkar : Actually, I haven't used it... I'm searching the information about this.. what about LiClO4, is it possible to use it at high potential?
i have tested 1 M LiPF6 in EC/DMC with LiNi1.5Mn0.5O2 between 3-4.9V, it shows no problem before 200 cycles although people say the solvent is not stable beyond 4.5 V. If you just want to test your cathode, you can do it, but long cycling should be not good because the electrolyte is being decomposed.