I want to dissolve FeCl3 in DMF with another organic compound to form a complex.
Materials:
- Iron(III) chloride (FeCl3)
- Dimethylformamide (DMF)
- Organic compound (ligand)
- Glassware and stirrer
Procedure:
1. Dissolve FeCl3** in DMF in a glass vessel. Use gentle heat if needed.
2. Add the organic compound** maintaining the desired ligand-to-metal ratio and stir. Heat may be applied to facilitate the reaction.
3. Observe changes** such as color shifts or precipitation indicating complex formation.
4. Isolate the complex** through filtration if precipitated or solvent extraction if dissolved.
5. Characterize the complex** using techniques like UV-Vis or IR spectroscopy.
Safety: Use PPE and handle all materials in a fume hood.
I think you have to try Ultrasonicator with a minimum temperature of 60 C.
Hi, I am using an Agilent 1200 series and Chemstation software. When I try to set run-time more than 40 mins (for ex. 45 mins or more than that), run-time is getting over within 40 mins even after...
26 January 2021 7,136 3 View
Hi, I'm trying to analyze a Kratky plot generated from my SAXS data. I am seeing multiple bell-shaped curves in my Kratky plot and I am not able to find any source to get relevant info on this...
20 January 2021 2,474 1 View
Hi, I'm doing 5/40nm In/Au e-beam evaporation at rates 0.2A/s(for In),1A/s(Au) on lithographically(doubly coated 495k,950k PMMA e-beam resist) done Si substrate at base pressure 2e-6torr. I'm...
18 January 2021 7,550 4 View
I am trying to import an Abaqus .inp file to Ansys but it does not import the whole assembly but only imports a single part. How to solve this.
17 January 2021 5,450 3 View
a PCR and gel electrophoresis was carried out to obtain the results. they are negative jak2 v617f samples (ref genome - NG_009904 )
13 January 2021 7,658 4 View
Since Abaqus CFD is no longer available in newer versions what are other available codes for Fluid-Structure Interaction Simulation
11 January 2021 2,012 3 View
I am studying about Impact load resistance property of Polyurea (Elastomer). With respect to this, I need to conduct tests on this material to evaluate its material model behavior as a...
29 December 2020 2,969 1 View
I have attached the files with this post to explain me how to remove rotation and center the origin at the body's local coordinate. This is just one sample and I have 1000s of files like this. I...
18 December 2020 3,838 3 View
Performed hydrothermal liquefaction of cellulose powder, at about 200 degrees for 10 16 hours. After simple filtration, I stored filtered product at room temperature for 4-6 days, there is the...
03 December 2020 7,327 3 View
My data for fungicide treated replication shows higher RMSE and R-square but less CV compared to the untreated replication for a regression between vegetation indices and yield. How correct is it?...
23 November 2020 2,079 6 View
I looking for ferro calcium production process
03 March 2021 1,755 4 View
I'm involved in a study of odor control technologies for municipal wastewater treatment plant. One of the control options involves a chemical 2-stage (acid/alkaline) packed bed scrubber. The...
03 March 2021 3,661 2 View
Hi all, I need to cleave the ester in Ethyl 2-amino-1H-imidazole-5-carboxylate to make the carboxylic acid and retrieve the product from solution to use in downstream applications of linking to...
01 March 2021 8,766 3 View
For example in one research article the Elemental analysis values of COF-TpPa-1 ( Triformylphloroglucinol (Tp) (63 mg, 0.3 mmol), Paraphenylenediamine (Pa-1) (48 mg, 0.45 mmol) are as follows...
24 February 2021 1,265 6 View
24 February 2021 1,005 1 View
I have used Picral etchant (4.2 g Picric acid, 10 mL Acetic acid, 70 mL Ethanol, 10 mL distilled water) but it didn't work. Is there any alternative?
21 February 2021 2,558 5 View
Hello, I am investigating properties of water in oil emulsion explosives. And adding hexamine (hexamethylenetetramine) into one of the phases that are used to make the emulsion should increase the...
21 February 2021 8,680 1 View
20 February 2021 8,202 6 View
Hi everyone, I am a teacher of Heterocycles Synthesis, Is there a home practice that you recommend for undergraduate students? A simulator would also be useful Due to the pandemic, students...
18 February 2021 2,769 4 View
I have done electrochemical impedance by using cyclic voltammetry for one organic material. from that, I plotted bode diagram. but actually, I am very confused about how to find the capacitive...
18 February 2021 3,023 3 View