I need polyaniline to be synthesized with a good yield by any chemical methods.
Hi. Thejas
Three major components are need for this synthesis.
1. 1 M Hcl 2. 1 M any Oxidizing agent like Ammonium peroxydisulfate or Ammonium Per sulfate etc 3. Aniline
step 1- You take 100 ml of 1M HCl and add to 5 ml of aniline, Keep on this mixture on magnetic stirrer.
Step 2. Add 100 ml of 1M Ammonium persulfate to above mixing solution drop wise, and keep these solution on magnetic stirrer for a period of 24 h.
Step 3. After 24h you get a dark green precipitate thats your polyaniline.
Step 4. now this precipitate is washed with distilled water till the ph comes normal range ( around ph=7.0) and collect polymerized Polyaniline.
Step 5. now this polyaniline put into a methanol solution and Dry in oven.
so this the way you can get a polyaniline with good yield.
Hope for the Best
Thanks
Also check this Review Paper "Some aspects of preparation methods and properties of polyaniline composites (Review)".
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