I am using Belsorp mini BET instrument. During the measurement, in the desorption stage, I face a message saying "V5 (F) needle valve is too tight" and the analysis interrupts.

I changed the V5 valve rang on the instrument to loosen the valve, but it did not help. Even I replaced the gas cylinder pressure regulator and the filter on measuring cells.

What would be the reason for such an error and how it can be resolved?

Thanks in advance.

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