I have no personal experience in making as-cast MMC with fly ash as the dispersant, but Professor P.K. Rohatgi does. His contact info is available at the end of the article attached. Good luck!
Aluminum-MMCs play a major role in the improvement of mechanical and tribological properties.It already proved that the tribological properties increases with the volume percentage of flyash content. "Fly-ash" from metallic-industry is desirable for making a reinforcement materials.