After preparation of Amino chalcones through Acylated Amino Acetophenone & benzaldehyde followed by base hydrolysis the product is gummy. i want to know
- if this is the nature of amino chalcone?
- how can i separate it effectively?
- how to increase the yield?
- suggested papers will be appreciated.
You can increase the yield by using ultrasonic bath ( sonication ).
thank you for your answer, but please specify how to use ultrasoncation to increase the yield?
Thank you.you can use ultrasonic cleaner (bath) insteate of reluxing ,heating and sterring.just hunging the reactants flask in the ultrasonic bath which contains water at r.t. it increases the yield and decrease the reaction time to minutes.It is very efficient for organometalic reactions and most of organic synthesizes.If you need more you can ask,please.
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