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I have taken 300mg of MWCNT, heated it for 3 hours under reflux in 100 ml of mixture acid (H2SO4 + HNO3) in a 3:1 ratio, and maintained the temperature at 95 degrees. I am using a PTFE membrane...
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Concentration used during functionalization was: sulfuric acid - 98wt% and nitric acid - 69-72 wt%.
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