01 January 1970 3 2K Report

I am trying to synthesize LiFePO4 but did not get success. I just copy many synthesis methods (by sol-gel and hydrothermal process) from reputed journals, still, i am not getting pure LiFePO4. Every time I did heat treatment in the iron tube furnace at 700 and 650 C in Argon atmosphere. Therefore I have a doubt that iron tube effecting the reaction. Because I am not getting proper XRD peaks. Please help me if anyone can give the reason.

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