I have prepared the TiO2 nanopowder by sol-gel method. In the FTIR spectra (% of transmission versus wavenumber) I was not able to get the peaks. Do you know what might be the reason or do you know of a alternative method?
peaks in FTIR of TiO2 includes Ti-Ti, Ti-O-Ti, O-Ti-O stretchings and vibrations. And other peaks will depend on type of precursors used and the solvent. Check your procedure of operation of your instrument and take reference properly.
Dear Mahnaz Alijai madam and Amit Kumar sir..the xrd of prepared nano TiO2 is confirmed..also the file no. 84-1286 is compared...then I should get the FTIR...I have discussed my friend today suggested KBR pellets must be used...I do not know the correct thing...plz suggest...