During the laboratory experiment of hydrocracking process, the experiment was set up at 16:43pm and the reaction temperature was 154C and pressure of hydrogen gas was 40bar. Then after 17:55pm temperature was increased to 166C and the liquid flow rate was 40mL/min. After temperature increased, the hydrogen sulphide gas was suddenly started to emit in the form of fume, while unconverted liquid which was on the bottom of heat exchanger or a chiller was completed black. My question is what would make the H2S to start emitted when temperature in the trickle bed reactor is increasing? And when temperature is constant H2S is not emitted?
Hy, again, Peter.
at this time I will suggest you two articles instead an answer. They are:
Asia Pacific Journal of Chemical Engineering, 2015, 10, p. 154-162, doi: 10.1002/apj1858 and
The Scientific World Journal, 2013, article ID739501, 8 p., doi10.1155/2013/739501.
i hope these articles help you.
best regards
Silas
Dear Dr. Derenzo,
Once again, thank you for your suggestion regarding to the articles.
Unfortunately, I do not have access with those articles you suggested. But I have send requested from two authors and I am waiting for their responding.
I hope I will find something uniques due to the problem I have found during the laboratory experiment.
Thank you for your time and support.
kind regards,
Peter Mponzi
Hi, Peter, they both are open journals, free on internet. I have attached them for you Good luck
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