I have synthesized some microporous ionic covalent organic frameworks, I collected their CO2 adsorption data at 273K, in order to calculate its QST, I wanna get some suggestions from the researchers in this field, that at what other temperatures I should analyze the CO2 adsorption in order to calculate QST? As well as please suggest me the amount of SO2 which is best to use for a breakthrough SO2 adsorption? As I already used up to 40mg sample for SO2 breakthrough experiment, is there any effect of the sample amount on SO2 breakthrough adsorption by microporous materials?
Another temperature of 25℃ （298K）can be employed for calculating QST. This referrence may be useful for you. Macromolecules 2014, 47, 5926−5931.
As regards for another question , i am sorry i have no idea to speak of.
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