Conductivity Vs 1000/T plot obtain from dynamic mode of measurement of Impedance spectra of the solid polymer electrolyte with active filler and salt shows a gradual dip at some certain range (35-46C) of temperature before melting event. However, for the same sample in a steady mode measurement , the conductivity shows VTF nature( not showing any decrease in conductivity). Both the experiment has been performed on same system with same heating rate.
Yes Sir, there is a distinct kink in the Arrhenius plot calculated at 1kHz ( in case of dynamic measurement) however for the same sample with same instrument it does not show any kink obtain at 1 kHz ( in case of static measurement). Both experiment are run at 1C/min using Hioki impedance analyzer.
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