It is related to heating the sample (solid material, inorganic salt) to a specific temperature. The explanation needs to clarify the main differences between thermal decomposition and calcination.
Dear Dr. Aimal Khan These terminologies could be differentiated based on the outcomes of the process. Calcination is the decomposition of a substance at high temp (below melting point) releasing volatile components under limited or no air conditions. While thermal decomposition is the thermal breakdown of particular materials into different products (like oxidation).
Thermal decomposition is the general process of breaking down a compound with heat, while calcination is a specific type of thermal decomposition that involves heating a substance to high temperatures in the absence of oxygen to produce oxides.
we say that thermal decomposition is broader term while calcination is a specific type of thermal decomposition