I'm trying to find a proper way to digest waste PCB samples for ICP analysis for measuring copper, gold, silver and palladium elements. I look forward for the answers of following questions:

1. How much grams of PCB samples are needed for digestion?

2. What acids needed to apply?

3. In what temperature all metals would be digested?

4. How can be sure that all metals being digested (considering some plastics and ceramics never solubilized by acids)?

5. What kind of vessel should be used for digestion?

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