I have to end a reaction in process due to sone emergency. I was synthesizing poly glycerol sebacate. I reacted them at 170 under nitrogen for an hr and then stopped. Normal duration is 4 hr. Should I continue it from ther or to go for new??
Dear Ramish Riaz, if kinetics consistency is important then you have to repeat the synthesis with respect to the reference procedure. You did not said any thing about evolved water elimination! Reversibility of the reaction by hydrolysis may occurs before restarting. My Regards
Dear Ramish Riaz, if kinetics consistency is important then you have to repeat the synthesis with respect to the reference procedure. You did not said any thing about evolved water elimination! Reversibility of the reaction by hydrolysis may occurs before restarting. My Regards
@Abdelkader BOUAZIZ i had attached condenser to eliminate produced water..
Dear Ramish Riaz, water can not be eliminated via a condenser, may be you mean a Dean-Stark. My Regards
You should fo it again, cause you Can not calculate the amount of the resulted water from the réaction if you keep it aside for a day
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