I am currently working on a research project where I need to synthesize calcium thioglycolate for further formulation studies.

I would appreciate detailed guidance on the following:

1. Reaction conditions – such as temperature, pH, and solvent considerations for optimal yield.

2. Stoichiometric ratios – precise amounts of calcium hydroxide (or other calcium sources) and thioglycolic acid needed for the reaction.

3. Purification and storage – best practices to ensure stability and prevent oxidation or degradation of the final compound.

4. Safety measures – since thioglycolic acid is reactive and can be hazardous, any important handling precautions would be helpful.

5. Authentic references – preferably published literature or reputable sources that describe the synthesis method.